Lesson
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🧯 Organophosphate Insecticides II

Additional organophosphate insecticides with emphasis on characteristics, toxicology, and safe handling.

This lesson introduces major organophosphate insecticides and summarizes their key chemical and practical characteristics.


PHORATE, PHOSALONE, DIMETHOATE AND QUINALPHOS

a) Phorate (Thimet)

(0, 0-diethyl-S-2-ethylthiomethyl phosphoro dithioate)

Derivative of Dithiophosphoric acid.

Phorate is produced by reacting dimethyl dithiophosphoric acid with

formaldehyde and ethyl mercaptan at room temperature.

The second method is by condensation of chloromethyl sulphide with sodium

dithiophosphoric acid.

Phorate is a clear liquid. B.P. 100°C, highly soluble in most organic solvents. It

is unstable to hydrolysis. In acid medium it is more stable. It is easily oxidized to the

corresponding sulphoxide which is resistant to hydrolysis and hence persists on plants

for long time providing insecticidal action.

Phorate has both systemic and contact insecticidal action and is a very toxic

compound. Phorate is absorbed and translocated in plants. It is oxidatively

metabolized. Phorate is employed for control of aphids, carrot fly, fruit fly and wire worm

in potatoes.

b) Phosalone (Zolone)

(0, 0-diethy-S-(6-chloro-2, 3-dihydro-2 oxobenzoxazol-3-yl) methyl

phosphorodithioate).

Derivative of Dithiophosphoric acid

Phosalone is a systemic insecticide and acaricide used in citrus and orchard

fruits. It is also used to control aphids in cereals, oilseed, rape and brassicas. It is also

used for testing seeds to protect the seedling from insect damage. LD50: 135 mg/kg.

Phosalone is produced by condensation of sodium or ammonium

diethyldithiophosphoate with 6-chloro-3 chloromethyl benzoxazolone.

It is practically insoluble in water. It is a white crystalline substance, m.p. 45

17°C. It is relatively stable in acid medium but in alkaline medium it is rapidly hydrolyzed

to the 6-chloro-benzenehexazolone diethyl thiophosphoric acid and formaldehyde.

c) Dimethoate (Rogor, phosphamide, cygon)

(0, 0-dimethyl-S-methyl carbamoylmethyl phosphoro dithioate).

Derivative of Dithiophosphoric acid

Dimethoate is a systemic and contact insecticides and acaricide, produced by

reacting salts of dimethyldithiophosphoric acid with N-methylchloroacetamide in aqueous

medium in the presence of some organic solvents.

It is also produced by reacting dithiophosphate with aqueous methylamine at low

temperature.

Pure dimethoate is a white crysatalline substance with camphor like odour. The

technical material is a yellowish brown (amber) coloured oily liquid with sulphurous acid

smell. It is highly soluble in water and most organic solvents. Dimethoate is thermally

unstable and on heating it decomposes.

d) Quinalphos (Ekalux) or (Bayrusil)

Derivative of Thiophosphoric acid.

Quinalphos (0, 0diethyl-0- (2-quinoxalinyl) phosphorothioate) is obtained by

condensation of 0-phenylenediamine with the hemi-acetal of glyoxylate.

The compound is highly active against biting and sucking insects and has an

LD50: 70 mg/kg rat (oral).

Quinalphos developed by Bayer AG (1969) is prepared by reaction of 0

phenylenediamine, chloroacetic acid and 0, 0-diethyl phosphorochloride thioate.

Quinalphos is a broad-spectrum contact and systemic insecticides, applied as

spray to control pests in cereals, brassicas and other vegetables. The mammalian

toxicity is quite high (LD50: 70 mg/kg) but the compound is degraded in plants within a

few days of application.


Summary Cheat Sheet

Topic Key exam point
Main class Organophosphates with emphasis on toxicology and safety
Common examples in lesson Phorate, phosalone, dimethoate, quinalphos
Mode of action AChE inhibition remains the common toxicological basis
Safety issue LD50, toxicity, and protective handling are major exam points
Antidote association Atropine is the classical antidote reference
Environmental point Persistence is lower than many organochlorines, but misuse still causes risk
Field caution Dose, timing, and protective gear are critical
Exam distinction Toxicology-focused OP questions differ from use/classification-focused OP questions
Poisoning clue Cholinergic symptoms are linked to OP poisoning
Trap Do not assume all organophosphates have identical hazard level or persistence

References

3 sources • [1] [2] [3]

[2]

Principles of Soil Science and Agricultural Chemistry — Standard BSc Agriculture Textbook

Book

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